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The book summarizes the available materials on the theory, technology, methodology, scope and prospects for the development of the most advanced method for the analysis of organic compounds --- capillary chromatography. Particular attention is paid to the issues of special requirements for chromatographic equipment and the peculiarities of the technique for preparing high-performance capillary columns. The questions of application of the method in chemical technology, in biomedical research, in the study of environmental pollution and in other areas are discussed. The book is intended for a wide range of scientific, engineering and technical workers, teachers, graduate students and university students.